最終更新日：2022/12/24
To synthesize TBDMS-dopamine methacrylate (TBDMS-DMA) monomer, methacryloyl chloride (0.46 g, 4.40 mmol) was added to TBDMS-dopamine (1.13 g, 2.96 mmol) in dichloromethane (2.5 mL) containing triethylamine (0.4 g, 4.0 mmol) according to the previously described method with modification. 35 The product was collected by precipitation.
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To
synthesize
TBDMS-dopamine
methacrylate
(TBDMS-DMA)
monomer,
methacryloyl
chloride
(0.46
g,
4.40
mmol)
was
added
to
TBDMS-dopamine
(1.13
g,
2.96
mmol)
in
dichloromethane
(2.5
mL)
containing
triethylamine
(0.4
g,
4.0
mmol)
according
to
the
previously
described
method
with
modification.
35
The
product
was
collected
by
precipitation.
